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The reaction mixture was stirred for a further 2 h at room temperature. The Ru1—N7 and N7—C10 bond lengths of 2. It appears that a rapid dissociation equilibrium occurs which leads to the formation of variable amounts of free imine plus other species. The three Ru—N Tp bond lengths: However, coordination of an imine on a metal fragment would be an important step in its activation toward nucleophilic attack or its hydrogenation reaction to give the amine.

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Originally Posted by WolvenArrow.

The molecular structure of I showing atoms numbering scheme. Special details clf Geometry. Refinement top Refinement on F 2 Primary atom site location: Reproduced material should be attributed as follows: R -factors based on F 2 are statistically about twice as large as those based on Fand R -factors based on ALL data will be even larger.

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All times are GMT CleanDevice has stopped working: For reproduction of material from all other RSC journals and books: Structure factor file CIF format https: Any help would be great. For related structures, see: Similar help and support threads. Similar help and support threads Thread Forum Driver for camera's Why oh why must I always reinstall the driver for my photo camera? We have observed that the benzophenone imine is lost readily in solution. On the other hand, despite the large number of known transition metal complexes containing multidentate imine ligands, the monodentate nitrogen-bond imine derivatives are rather rare Albertin et al.

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An approximate isotropic treatment of cell s. Go to our Instructions for using Copyright Clearance Center page for details. Untitled Document They don't see to work for me, goes to this link: The three Ru-N Tp bond lengths [2.

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You do not have JavaScript enabled. Back to tab navigation Download options Please wait The synthesis of the title compound I was carried out as follows: The mixture was heated using a warm water bath for 30 min. Back to tab navigation. In complex Ithe environment about the ruthenium metal center corresponds to a slightly distorted octahedron and the bite angle of the Tp ligand produces an average N—Ru—N angle of The time now is Driver for camera's Why oh why must I always reinstall the driver for my photo camera?